1. 在ICP開機前和過程中,務(wù)必翻開空調(diào)保證室溫固定在22℃,以免光學(xué)元件受溫度變化影響產(chǎn)生譜線漂移,形成測定數(shù)據(jù)不穩(wěn)定。
1. Before and during the start-up of ICP, it is necessary to turn on the air-conditioner to ensure that the room temperature is fixed at 22 C, so as to avoid the spectral drift of optical elements affected by temperature changes and unstable measurement data.
2.在ICP開機前和過程中,視狀況翻開抽濕機,確保室內(nèi)濕度控制在45%~60%之間,以免過大的濕度影響高頻發(fā)射器,輕則等離子體不易點燃,重則高壓擊毀元件,損壞高頻發(fā)射器及電路主板。
2. Turn on the dehumidifier according to the condition before and during the start-up of ICP to ensure that the indoor humidity is controlled between 45% and 60%, so as to avoid excessive humidity affecting the high-frequency transmitter, light plasma is not easy to ignite, heavy high-voltage destroys components and damages the high-frequency transmitter and circuit motherboard.
3.在ICP開機前和過程中要翻開抽風系統(tǒng),掃除工作時產(chǎn)生的有毒氣體,防止有毒氣體留在室內(nèi),對人員安康形成危害。
3. Before and during the start-up of ICP, the exhaust system should be turned on to clean up the toxic gases produced during the work, so as to prevent the toxic gases from remaining indoors and causing harm to people's health.
4.要經(jīng)常除塵和防塵。在斷開電源的狀況下,用枯燥干凈的紗布或者小毛刷或者吸塵器將各個部位的積塵清算潔凈。
4. Dust removal and prevention should be frequent. When the power supply is disconnected, the dust deposits in various parts are cleaned by dry and clean gauze or small brush or vacuum cleaner.
5.ICP要運用高純氬氣,純度請求99.99%以上,以免形成點不著火或者ICP熄滅。
5. ICP should use high purity argon with purity over 99.99% to avoid ignition or ICP extinguishing.
6.ICP工作中確保氣流穩(wěn)定。留意不要讓管子彎曲太兇猛,以免載氣流量不穩(wěn)定形成脈動,影響測定。并且在ICP工作中經(jīng)常察看減壓閥,保證氬氣壓力在0.6~0.7MPa。
6. Ensure airflow stability in ICP work. Be careful not to bend the pipe too fiercely, so as to avoid the fluctuation of carrier gas flow and influence the measurement. In ICP work, pressure relief valves are often inspected to ensure that the argon pressure is between 0.6 and 0.7 MPa.
7.要定期清洗霧化器和炬管。特別是測定高鹽溶液之后,不及時清洗,會形成 霧化器梗塞,炬管噴嘴積有的鹽分會形成氣溶膠通道不正常。要定期用稀硝酸、去離子水洗。
7. Clean atomizer and torch tube regularly. Especially after the determination of high salt solution, if it is not cleaned in time, the atomizer obstruction will be formed, and the aerosol channel will be abnormal if the salt accumulated in the nozzle of the torch tube. Wash regularly with dilute nitric acid and deionized water.
8.開機測定前,要事前布置好各項準備工作,切忌短暫的時間距離里開開停 停,防止儀器頻繁開啟形成損壞。由于儀器每次開機時,瞬時電流大大高于正常工作電流,瞬時的脈沖沖擊容易形成功率燈絲斷絲,碰及短路等。
8. Before startup test, all preparatory work should be arranged beforehand. Do not start or stop in a short time interval to prevent damage caused by frequent opening of the instrument. Because the instantaneous current is much higher than the normal working current when the instrument is turned on each time, the instantaneous impulse impulse is easy to cause the power filament to break, touch and short circuit.
9.每次完成實驗,確保樣品溶液、規(guī)范溶液遠離儀器,減少揮發(fā)對儀器的腐蝕。
9. Complete the experiment every time to ensure that the sample solution and standard solution are far away from the instrument and reduce the corrosion of volatilization to the instrument.
10.循環(huán)冷卻水要用蒸餾水,避免結(jié)垢。
10. Distilled water should be used for circulating cooling water to avoid scaling.
11.長時間不運用時,每周要開機一次,每次少到達30min以上。
11. When not in use for a long time, turn on the machine once a week, at least 30 minutes at a time.
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